HomeMy WebLinkAbout1998-070 Report - Reeder PistolReport
Sampling and Analysis Results,
Reeder Pistol Range,
Ashland, Oregon
Prepared for
City of Ashland
May 1998
Prepared by
CH2MHILL
POX17D9D.DOC
Contents
Section Page
Introduction .........................................................................................................................................1
Sample Collection ................................................................................................................................1
Site Cleanup Levels .............................................................................................................................1
Analytical Results ................................................................................................................................3
Shooting and Separation Lanes ............................................................................................3
Area North of Shooting Lanes ..............................................................................................5
Range Berm .............................................................................................................................5
Waste Classification ............................................................................................................................6
Conclusions ..........................................................................................................................................6
Recommendations ...............................................................................................................................6
Excavation ...............................................................................................................................7
Confirmation Sampling .........................................................................................................7
Additional Excavation ...........................................................................................................7
Waste Disposal .......................................................................................................................7
Appendix
A Laboratory Reports
Tables
Shooting and Separation Lane Analytical Results ...............................................................3
Area North of Shooting Lane Analytical Results .................................................................5
Range Berm Analytical Results ...............................................................................................5
Figures
Berm, Shooting Lane, and Separation Lane Sample Locations ..........................................2
Soil Sample Lead Concentrations ...........................................................................................4
Flow Chart Managing Soil as a Hazardous Waste ...............................................................8
Flow Chart for Onsite Soil Treatment ....................................................................................9
PDX17D9D.DOC
Introduction
This report presents the results of the April 22, 1998, soil sampling and analytical testing for
the Reeder Pistol Range in Ashland, Oregon. Samples were collected as described in the
Sampling and Analysis Plan, Reeder Pistol Range, Ashland, Oregon, CH2M HILL, February 1998
(SAP). The sample results were then compared to State of Oregon soil cleanup levels. Based
on the analytical results, recommendations for future site cleanup are also included in this
report.
Sample Collection
A total of 60 soil samples were collected from the range berm, shooting lanes, and an area
north of the shooting lanes. Samples were collected from the following locations:
· At the ground surface, 1-foot, and 2-foot depth below ground surface (bgs) from 10
locations in the shooting lanes and 5 locations in the area north of the shooting lanes
· Three locations along the range berm at the berm surface and every 2 feet horizontally
toward the center of the berm to a distance of 8 feet
Figure 1 shows the sample station locations.
Subsurface and range berm sample locations were collected from test pits dug with a
backhoe. Ron Kinney, a subcontractor to the City of Ashland, provided the backhoe and
performed the excavation work.
The excavations were approximately 3 feet wide by 2.5 feet deep to allow access into the test
pits. Soil samples were then collected from the side walls of the excavations using new
stainless steel spoons. The spoons were clean prior to use and were discarded after each
sample was collected to prevent cross contamination of the soil samples.
Samples were labeled using the following nomenclature: XXYY-D-Z
Where:
XX = Site area designator:
RB = Range Berm
SL = Shooting Lane
NA = Area North of Shooting Lanes
YY = Sequential sample station location
D -- Depth in feet from which sample was collected below ground surface or
distance from face of berm toward center of berm
Z = V, if verification sample location, otherwise left blank
Site Cleanup Levels
No site cleanup level for lead has been established for the site. However, as an initial
evaluation of the site soils that could require corrective action, the analytical results were
PDX17D9D.DOC
/ ® NA12
/
/
/
/
/ · NA11
iI
Asphalt Pad '~
· NA10
Legend
Sample Location
(typical)
Not to Scale
· Soil Sample Location
· Berm Sample Location
· Verification Sample Location
Clearing/Tree Line
Edge of Berm ~ ... --' '/
Samples at the range berm aerm Cross Section
surface and every 2 feet
horizontally towards the center
of the berm to a maximum
distance of 10 feet
Figure 1
Berm, Shooting Lane and Separation
Lane Sample Locations
Reeder Pistol Range, Ashland Oregon
~ CH2MHILL
SAMPLING AND ANALYSIS RESULTS, REEDER PISTOL RANGE
compared to the State of Oregon lead soil cleanup level for residential sites of 200 milli-
grams per kilogram (mg/kg) provided in OAR 340-122-045. This cleanup level is considered
protective of children when exposed to soils of this lead concentration in a residential
exposure scenario. The residential cleanup level is the most conservative of the generic soil
cleanup levels used by the Oregon Department of Environmental Quality (DEQ).
Analytical Results
A total of 60 samples were submitted to CH2M HILL Analytical Services in Corvallis,
Oregon. Select samples were chosen for analysis using the phased approach described in the
SAP. Of the 60 samples collected, 29 were chosen for Phase I total lead analysis using EPA
Method 6010B, as described in the SAP. The samples that were not analyzed were held by
the laboratory for potential future analysis (Phase II analysis). If Phase ! samples exhibited
concentrations of lead exceeding the DEQ residential cleanup level of 200 mg/kg, then
select Phase II samples would have been analyzed to better delineate the extent of lead
present on site.
The analytical results are summarized on Figure 2. Laboratory reports for the analytical
results are provided in Appendix A and are discussed in the following subsechons.
Shooting and Separation Lanes
A total of 12 samples collected from the shooting and separation lanes were selected for
Phase I analysis. All samples analyzed from the surface and 1 foot bgs were below the
method detection limit, which was less than 10.7 mg/kg. Since no sample exceeded the
200 mg/kg residential cleanup level for lead, no Phase II sample analyses were necessary.
Table 1 summarizes the analytical results for Phase I samples analyzed from the shooting
and separation lanes.
TABLE 1
Shooting and Separation Lane Analytical Results
Reeder Pistol Range, City of Ashland
Sample Depth Lead
Sample Station Sample I.D. (feet) (mg/kg)
SL1 SLI-O 0 non detect (< 10.7)
SL1 SLI-1 1 non detect ( < 9.8)
SL2 SL2-O 0 non detect (< 7.3)
SL2 SL2-1 I non detect (< 7.9)
SL5 SL5-O 0 non detect (< 7.2)
SL5 SL5-1 1 non detect (< 10.4)
SL6 SL6-O 0 non detect (< 6.5)
SL6 SL6-1 1 non detect (< 7.2)
SL14 SL14-O-V 0 non detect (< 6.5)
SL14 SL14-1-V 1 non detect (< 9.4)
SL15 $L15-O-V 0 non detect (< 8.1)
SL15 SL15-1 -V 1 non detect (< 10.4)
PDX17D9D.0OC 3
Depth
(. ~s)
Surface
1
Legend
/ Sample NA12
/' Lead
~ .- ..- --~ (ft bgs) (rnoJkg)
/Surface ND
/ 1 ND
/ Sarn~e NA11
/ Lead
/ ~ Depth ~on
// A ~ (~ bgs) (moJkg)
I ND.
Sample
Concent~on ~ (it bgs)
(rnoJkg)~
ND '" ~ ·
ND \
Sample: SL6
Lead
Depth Concentration
(ft bgs) (mg/kg) \
Surface ND \
I ND \
Sample SL15 \
Lead
Depth Concentration
(ft bgs) (mg/kg) \
Surface ND \
1 ND \
Sample SL14 \
Lead
Not to Scale
(mg/kg)
ND
ND
'\
DepthClearing/Tree Line
(ft bgs)
\ 1
Sarnl:~e
m bgs)
(mg~,g)
ND
ND
SL1
- (moJkg)
ND
ND
Depth Concentration \ / Lead
(ft bgs) (rng/kg) \ ,a / "'"' Depth ~ration
Surface ND \. ,& "~/ (it bgs) (mg/kg)
I IND 'x ~,/'~ Surface NO
Edge of Berm \ .~- / ~
\ . / '~ / Sample RB16
Sample RB 18 .~/- '" / Lead
Lead ~ / Depth Concentration
Depth Concentration ~ ~ (ft bas) ('ma a~
.......... /k~.
(ft bgs) (mg/kg) ~bamp~e RB 1! Surface 62.3
Surface 9,370 Lead 1 ND
I ND Depth Concentration
2 43.5
2 ND (ft bgs) (mg/kg)
Surface 2,610
1 ND
2 ND
Note: Not all sample locations were analyzed because of phased sample approach
ND Non Detect for Lead; Detection Limit <12 mg/kg For All Samples
· Soil Sample Location
· Berm Sample Location
· Verification Sample Location
Figure 2
Soil Sample Lead Concentrations
Reeder Pistol Range, Ashland Oregon
~ CH2MHILL
SAMPLING AND ANALYSIS RESULTS, REEDER PISTOL RANGE
Area North of Shooting Lanes
A total of eight samples collected from the area north of the shooting lanes were selected for
analysis. All samples analyzed from the surface and 1 foot bgs were non-detect at a detec-
tion limit of less than 11.2 mg/kg. No Phase II sample analyses were necessary to delineate
the extent of lead present in the area north of the shooting lanes. Table 2 summarizes the
analytical results for Phase I samples analyzed from the area north of the shooting lanes.
TABLE 2
Area North of Shooting Lane Analytical Results
Reeder Pistol Range, City of Ashland
Sample Depth Lead
Sample Station Sample I.D. (feet) (mg/kg)
NA9 NA9-0 0 non detect (< 7.8)
NA9 NA9-1 1 non detect (< 8.0)
NA1 1 NA1 1-0 0 non detect (< 6.5)
NA11 NA1 1-1 1 non detect (< 11.2)
NA12 NA12-0 0 non detect (< 9.7)
NA12 NA12-1 1 non detect (< 7.5)
NA13 NA13-0 0 non detect (< 9.5)
NA13 NA13-1 1 non detect (< 8.1 )
Range Berm
A total of nine samples collected from the range berm were selected for analysis. The
maximum concentration of lead detected at the surface of the berm face was 9,370 mg/kg.
Interior berm samples collected at horizontal distances of 2 feet and 4 feet into the berm
exhibited a maximum lead concentration of 43.5 mg/kg. No Phase II sample analyses were
necessary to delineate the extent of lead present in the berm. Table 3 summarizes the
analytical results for Phase I samples analyzed from the range berm.
TABLE 3
Range Berm Analytical Results
Reeder Pistol Range, City of Ashland
Sample Distance into Berm Lead
Sample Station Sample I.D. (feet) (mg/kg)
RB16 RB16-0 0 62.3
RB16 RB16-2 2 non detect (< 7.8)
RBt6 RB16-4 4 43.5
RB17 RB17-0 0 2,610
RB17 RB17-2 2 non detect (< 7.3)
RB17 RB17-4 4 non detect (< 8.2)
RB18 RB18-0-V 0 9,370
RB18 RB18-2-V 2 non detect (< 10.2)
RB18 RB18-4-V 4 non detect (< 9.0)
PDX17D9DDOC 5
SAMPLING AND ANALYSIS RESULTS, REEDER PISTOL RANGE'
Waste Classification
The two soil samples from the surface of the berm that exceeded the 200 mg/kg residential
cleanup level (RB18-0-V and RB17-0) were analyzed using the toxicity characteristic leaching
procedure (TCLP, EPA Method 1311) to characterize leachate concentrations. The TCLP test
method was established by the Environmental Protection Agency (EPA) to simulate what
might occur if the soil was placed in a solid waste landfill. TCLP lead analytical results for
RB18-0-V and RB17-0 were 79.6 milligrams per liter (mg/L) and 59.8 mg/L, respectively.
Soil exceeding 5 mg/L per TCLP lead is classified as a characteristic hazardous waste
because it exhibits the toxicity characteristic and carries the waste code D008.
Conclusions
Lead was detected at concentrations exceeding the DEQ residential cleanup level in two of
the three samples collected along the face of the berm. The results indicate that it is likely
that the soil in the outer I foot of the berm face will contain lead at concentrations greater
than the DEQ residential cleanup level of 200 mg/kg.
Lead is present at concentrations below the DEQ residential cleanup level in the shooting
and separation lanes and the area north of the shooting lanes. In addition, lead
concentrations in the interior of the berm did not exceed the DEQ residential cleanup level.
These results indicate that lead at levels of potential concern is concentrated in the surface of
the range berm. The data do not indicate that lead-affected soils have migrated to other
areas of the pistol range.
TCLP results for soils from the surface of the range berm indicate that these soils are a
characteristic hazardous waste as defined by Chapter 40 of the Code of Federal Regulations
(CFR) Part 261.24.
Recommendations
CH2M HILL recommends a limited removal action involving excavation and offsite
disposal of soil containing lead at concentrations greater than the DEQ residential cleanup
level. Analytical results indicate that the target cleanup level of 200 mg/kg for lead can be
achieved by removing the upper 1 foot of the berm face. CH2M HILL estimates that
approximately 30 cubic yards of soil would require removal and offsite disposal.
There are two approaches to initiate this removal action:
Excavate I foot of soil from the face of the range berm, collect confirmation samples to
confirm that the residual soils meet the cleanup standard, transport soils to an offsite
facility for treatment as a hazardous waste, and dispose of treated soils in a solid waste
landfill. This approach requires that the City prepare a hazardous waste manifest for soil
transportation and offsite treatment. An EPA hazardous waste generator ID number is
required for the manifest (40 CFR Part 262).
· Excavate I foot of soil from the face of the range berm, collect confirmation samples to
confirm that the residual soils meet the cleanup standard, treat soils onsite so they are no
PDX17D9D.DOC 6
SAMPLING AND ANALYSIS RESULTS, REEDER PISTOL RANGE
longer classified as a hazardous waste, and dispose of treated soils in a solid waste
landfill. This approach requires that the City enter the DEQ Voluntary Cleanup
Program.
Figures 3 and 4 present flow charts for these two approaches. The remainder of this section
presents a more detailed description of these two approaches.
Excavation
The general excavation strategy for both approaches will be to excavate the upper I foot of
the berm face, collect confirmation samples from the exposed berm face, and perform
additional excavation if confirmation sampling indicates that lead remains present at
concentrations greater than the target cleanup level.
Confirmation Sampling
After excavating the upper 1 foot of the berm face, confirmation samples will be collected
from the exposed berm face to demonstrate that the soil excavation effort has met the goal of
removing soil above the cleanup level. Confirmation samples will be analyzed for total lead
using EPA Method 6010 to demonstrate compliance with the 200 mg/kg lead cleanup
criterion.
Representative samples will be collected from the exposed face of the berm every 10 feet
along the face of the berm at a height of 4 feet above the shooting lane grade.
Additional Excavation
In the event that a representative sample of the exposed berm face exceeds the cleanup
criterion, the excavation will be deepened an additional foot in the area of that sample. For
example, if one sample exceeds the cleanup criterion and the samples to either side of it are
below the cleanup criterion, the excavation will be deepened 1 foot from the exceeding
sample to half the distance to the next adjacent sample below the cleanup criterion.
Waste Disposal
The soil that is present in the upper foot of the berm face is assumed to be a characteristic
hazardous waste based on the initial TCLP results. Soil exhibiting lead as a characteristic
hazardous waste must either be transported as a hazardous waste or treated prior to
transportation to be hauled as a solid waste. These two alternatives are discussed in the
following sections.
Alternative 1 - Manage Soil as Hazardous Waste
This alternative would consist of excavating the soil, loading the soil directly into transfer
trucks, and hauling the soil to an offsite treatment facility. The material would be
manifested as a hazardous waste for offsite soil treatment.
The soil will ultimately be disposed of in a Subtitle D landfill. The excavated soil will be
stabilized at the disposal facility by mixing a reagent such as a cement or kiln dust slurry
with the soil to reduce leachable lead concentrations to less than 5 mg/L.
PDX17D9O.DOC 7
Excavate 1-foot of soil from
face of berm
Collect confirmation samples
from face sides of
excavation
Yes
Transport material as a
hazardous waste for offsite
treatment. Place soil in a
Subtitle D landfill.
No
Excavate an additional
6 inches in areas of
exceedance
Figure 3
Flow Chart Managing Soil as a
Hazardous Waste
Reeder Pistol Range, Ashland, Oregon
~ CH2MHILL
Enter DEQ Voluntary
Cleanup Program to Treat a
Hazardous Waste
Excavate 1 -foot of soil from
· face of berm
Collect confirmation samples Confirmati~
· from face sides of '"- concentratio~%~~~ ~- Stop Excavation
excavation Yes
·
No
Excavate an additional
6 inches in areas of
exceedance
Analyze representative ,~ Transport stabilized soils as
sample for TCLP lead v a solid waste and place in a
Subtitle D landfill
~ ~. Stabilize excavated soils in
I-- drop boxes
No
Figure 4
Flow Chart For Onsite Soil Treatment
Reeder Pistol Range, Ashland, Oregon
'~i~ CH2MHILL
SAMPLING AND ANALYSIS RESULTS, REEDER PISTOL RANGE
Soil will be transported to the treatment facility using transport trucks designed to carry
hazardous wastes. Each load will be transported under a properly executed hazardous
waste manifest accompanied by a bill of lading and a copy of the laboratory analysis report
representative of soil.
Alternative 2 - Treat Soil Onsite, Haul and Dispose as a Solid Waste
This alternative would consist of excavating the soil as described above. The excavated soil
would be placed directly in drop boxes where the soil would be stabilized by adding
cement, and hauling the treated soil to a Subtitle D landfill for disposal. However, to
stabilize a hazardous material onsite, the City of Ashland would first need to enter into the
DEQ Voluntary Cleanup Program to qualify for exemption from Resource Conservation and
Recovery Act (RCRA) rules.
The stabilized soil would then be sampled and analyzed for TCLP lead to confirm that the
leachable lead concentration did not exceed 5 mg/L. If the TCLP lead confirmation sample
failed the 5 mg/L criterion, the stabilization procedure would be repeated.
Soil will be transported to the Subtitle D landfill in the drop boxes via truck. Each load will
be transported under a properly executed nonhazardous waste manifest accompanied by a
bill of lading and a copy of the laboratory analysis report representative of soil.
PDX17D9D.DOC 10
APPENDIX A
Laboratory Reports
PDX17D9D.DOC
CH2MHILL
iAnalytical Services
Cli2M HILL
Analytical Servic~
2300 NW Walnut Bird
Corvallis, OR
97330-3538
P.O. Box 428
Corvallis, OR
973394~428
Tel 541.752.4271
Fax 541.752.0276
May 6, 1998
Reeder
145794.SA.01
RE:
Analytical Data for Reeder
CVO Laboratory Reference No. 7158
Steve O'Malley/PDX
On April 23, 1998, CH2M HILL Corvallis Analytical Services received sixty samples with a
request for analysis of selected parameters.
The analytical results and associated quality control data are enclosed. Any unusual
difficulties encountered during the analysis of your samples are discussed in the case
narrative.
Under CH2M HILL policy, your samples will be stored for 30 days after reporting. If you
have not given us prior instructions for disposal, we will contact you if any samples require
disposal as hazardous waste.
CH2M HILL Corvallis Analytical Services appreciates your business and looks forward to
serving your analytical needs again. If you should have any questions concerning the data, or
if you need additional information, please call Ms. Kathy McKinley at (541) 758-0235,
extension 3120.
Sincerely,
Kelly Ensor
Senior Administrative Assistant
Enclosures
Client/Project: Reeder
I.
Holding Time:
All acceptance criteria were met.
II. Digestion Exceptions:
None
III. Analysis:
IV.
CASE NARRATIVE
METALS
Lab Reference No.: 7158
go
Calibration:
All acceptance criteria were met.
Blanks:
All acceptance criteria were met.
ICP Interference Check Sample:
All acceptance criteria were met.
Spike Sample(s):
All acceptance criteria were met.
Duplicate Sample(s):
All acceptance criteria were met.
Laboratory Control Sample(s):
All acceptance criteria were met.
ICP Serial Dilution:
Not Required.
H. Other:
None
Documentation Exceptions:
None
I certify that this data package is in compliance with the terms and conditions agreed to by the
client and CH2M HILL, both technically and for completeness, except for the conditions detailed
above. Release of the data contained in this hardcopy data package has been authorized by the
Laboratory Manager or his designee, as verified by the following signature.
Prepared by:
Reviewed by:
CH2M HILL Analytical Services
Client Information
Project Name: Reeder
Project Manager: Steve O'Malley/PDX
Sampled By: S. O'Malley
Sampling Date: 04/22/98
Type: Grab
Matrix: Soil
Basis: Dry Weight
Lab Information
Date Rec'd: 04/23/98
Batch ID: 7158
Report Revision No.: 0
Reported By: L. Larsson
Reviewed By:.
Analyte: Lead, Pb by ICP
Method: 6010B
Units: mg/kg
Client ID Lab ID
SL1-0 715801
SLI-1 7158O2
SL2-0 715804
SL2-1 7158O5
SL5-0 715813
SL5-1 715814
SL6-0 715816
SL6-1 715817
NA9-0 715825
NA9-1 715826
NA11-0 715831
NA11-1 715832
NA12-0 715834
NA12-1 715835
NA13-0-V 715837
NA13-1 -V 715838
SL14-0-V 715840
SL14-1 -V 715841
SL15-0-V 715843
SL15-1-V 715844
RB16-0 715846
RB16-2 715847
RB16-4 715848
RB17-0 715851
RB17-2 715852
RB17-4 715853
RB18-0-V 715856
RB18-2-V 715857
RB18-4-V 715858
Reporting Sample Date
Limit Result Analyzed
10.7
9.8
7.3
7.9
7.2
10.4
6.5
7.2
7.8
8.0
6.5
11.2
9.7
7.5
9.5
8.1
6.5
9,4
8.1
10.4
10.0
7.8
8.2
8.5
7.3
8.2
7.0
10.2
9.0
10.7 U 05/O5/98
9.8 U 05/05/98
7.3 U 05/O5/98
7.9 U 05/05/98
7.2 U 05/O5/98
10.4 U 05/05/98
6.5 U 05/05/98
7.2 U 05/05/98
7.8 U 05/05/98
8.0 U 05/05/98
6.5 U 05/05/98
11.2 U 05/05/98
9.7 U O5/O5/98
7.5 U 05/05/98
9.5 U 05/05/98
8.1 U 05/05/98
6.5 U 05/05/98
9.4 U O5/O5/98
8.1 U 05/05/98
10.4 U 05/05/98
62.3 05/05/98
7.8 U 05/05/98
43.5 05/05/98
2610 05/05/98
7.3 U 05/05/98
8.2 U 05/05/98
9370 05/05/98
10.2 U 05/05/98
9.0 U 05/05/98
U=Not detected at specified reporting limits
CH2M HILL 2300 NW Walnut Blvd., Corvallis, OR 97330-3538 Tel 541.752.4271
Analytico; Services P.O. Box 428, Corvallis, OR 973390428 Fax 54 1.752.0276
CH2MHILL Analytical Services
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AND AGREEMENT TO PERFORM SERVICES
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Project #
Project Name
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Company Name
Project Manager or Contact & Phone
Requested Completion Date: Site ID
Purchase Order #
Report Copy to:
¢---- S,'&¢"~
Sample Disposal:
D ?{~e Return
CLIENT SAMPLE ID LAB
(9 CHARACTERS) QC
F~ LRD 5090 Caterpillar Road
Redding, CA 96003-1412
(916) 244-5227 FAX (916) 244-4109
Type Matrix
C G W S A
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M A T I R
P B E L
Date Time R
5' &..L -
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Sampled By and Title ",- (Please sign and print name) Date/rime Relinquished By
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Requested Analytical Method #
Preservative
COC # [ '
THIS AREA FOR LAB USE ONLY
Lab # Page o~.~
Lab PM Custody Review
Log In LIMS Verification
pH Custody Seals
Ice
QC Level ~) 2 3 Other
Cooler Temperature ~-'
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CH2MHILL Analytical Services
CHAIN OF CUSTODY RECORD
AND AGREEMENT TO PERFORM SERVICES
~ LM6 2567 Fairlane Drive
Montgomery, AL 36116-1622
(334) 271-1444 FAX (334) 27%3428
L~ LRD 5090 Caterpillar Road
Redding, CA 96003-1412
(916) 244-5227 FAX (916) 244-4109
~3 LKW Canviro Analytical Laboratories, fnc.
50 Bathurst, Unit 12, Waterloo, Ontario, Canada N2V 2C5
(519) 747-2575 FAX (519) 747-3806
Project # Purchase Order #
Project Name
Company Name
Project Manager or Contact & Phone 8 Report Copy to:
Requested Completion Date: Site ID Sample Disposal:
Type ~atrlx
C G W S A
Sampling O R A O ~ CLIENT SAMPLEID LAB
M A T ~ R (9 CHARACTERS) QC
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Date Time R
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Sampled By and Title . (Plt~ase sign and print name} Date/Time
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UPS Fed-Ex
Special Instructions:
Preservative
{ ,
~ "4
x'
Received By
Relinquished By
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[] CV0 2300
Nw Walnut Boulevard
Corvallis, OR 97330-3638
(541)752-4271 FAX (541) 752-0276
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THIS AREA FOR LAB USE ONLY
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CH2MHILL Analytical Services
CHAIN OF CUSTODY RECORD
AND AGREEMENT TO PERFORM SERVICES
L~ LMO 2567 Fairlane Drive
Montgomery. AL 36116-1622
(334) 271-1444 FAX (334) 271-3428
[] LRD 5090 Caterpillar Road
Redding, CA 96003-1412
(916) 244-5227 FAX (916) 244-4109
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L~ LKW Canviro Analytical Laboratories, Inc.
50 Bathurst, Unit 12, Waterloo, Ontario, Canada N2V 2C5
(519) 747-2575 FAX (519) 747-3806
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(541) 752-4271 F~(541) 752-0276
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Log In LIMS Verification
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CH21VlHILL Analytical Services
CHAIN OF CUSTODY RECORD
AND AGREEMENT TO PERFORM SERVICES
~ LM(~ 2567 Fairlane Drive [] LRD 5090 Caterpillar Road ~ LKW Canviro Analytical Laboratories, 1no. [] CV0 2300 NW Walnut Boulevard
Montgomery, AL 36116-1622 Redding, CA 96003-1412 50 Bathurst, Unit 12, Waterloo, Ontario, Canada N2V 2C5 Corvallis, OR 97330-3638
(334) 271-1444 FAX (334) 271-3428 (916) 244-5227 FAX (916) 244 4109 (519) 747-2575 FAX (519) 747-3806 (541) 752-4271 FAX (541) 752-0276
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CH2MHILL Analytical Services
CHAIN OF CUSTODY RECORD
AND AGREEMENT TO PERFORM SERVICES
E~ I. M6 2567 Fairlane Drive
Montgomery, AL 36116-1622
(334) 271-1444 FAX (334) 271-3428
I~l LRD 5090 Caterpillar Road
Redding, CA 96003-1412
(916) 244-5227 FAX (916) 244 4109
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[] LKW Canviro Analytical Laboratories, Inc.
50 Bathurst, Unit 12, Waterloo, Ontario, Canada N2V 2C5
(519) 747-2575 FAX (519) 747-3806
Requested Analytical Method #
Preservative
Special. Instructions:
Relinquished By Empty Bottles Date/Time Received By
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[] CVO 2300 NW Walnut Boulevard
Corvallis, OR 97330-3638
(541)752-4271 F~..)(541) 752-0276
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Lab #
Log In
pH
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CH2MHILL
Analytical Services
CII2M HILL
Analytical Services
2300 NW Walnut Bird
Corvallis, OR
97330-3538
P.O. Box 428
Corvallis, OR
97339-0428
Tel 541.752.4271
Fax 541.752.0276
May 18, 1998
Reeder
145794.SA.01
RE:
Analytical Data for Reeder
CVO Laboratory Reference No. 7158
Steve O'Malley/PDX
On April 23, 1998, CH2M HILL Corvallis Analytical Services received sixty samples with a
request for analysis of selected parameters. On May 11, 1998, additional analyses were
requested on samples 7158-51 and 7158-56.
The analytical results and associated quality control data for the TCLP Lead are enclosed.
Any unusual difficulties encountered during the analysis of your samples are discussed in the
case narrative.
Under CH2M HILL policy, your samples will be stored for 30 days after reporting. If you
have not given us prior instructions for disposal, we will contact you if any samples require
disposal as hazardous waste.
CH2M HILL Corvallis Analytical Services appreciates your business and looks forward to
serving your analytical needs again. If you should have any questions concerning the data, or
if you need additional information, please call Ms. Kathy McKinley at (541) 758-0235,
extension 3120.
Sincerely,
Kelly Ensor
Senior Administrative Assistant
Enclosures
Client/Project: Reeder
I.
II.
III.
IV.
Prepared by:
Reviewed by:
CASE NARRATIVE
METALS
Lab Reference No.: 7158
Holding Time:
All acceptance criteria were met.
Digestion Exceptions:
None
Analysis:
A. Calibration:
All acceptance criteria were met.
B. Blanks:
All acceptance criteria were met.
C. ICP Interference Check Sample:
All acceptance criteria were met.
D. Spike Sample(s):
All acceptance criteria were met.
E. Duplicate Sample(s):
All acceptance criteria were met.
F. Laboratory Control Sample(s):
All acceptance criteria were met.
G. ICP Serial Dilution:
Not Required.
H. Other:
None
Documentation Exceptions:
None
I certify that this data package is in compliance with the terms and conditions agreed to by the
client and CH2M HILL, both technically and for completeness, except for the conditions detailed
above. Release of the data contained in this hardcopy data package has been authorized by the
Laboratory Manager or his designee, as verified by the following signature.
Corvallis Analytical Services Laboratory
Client Information
Project Name: Reeder
Project Manager: Steve O'Malley/PDX
Sampled By: S. O'Malley
Sampling Date: 04/22/98
Type: Grab
Matrix: TCLP extraction fluid
Basis: Extracted
Lab Information
Date Rec'd: 04/23/98
Batch ID: 7158
Method: EPA1311/SW6010B
Report Revision No.: 0
Reported By: K. DJ~/~LALA
Reviewed B y.~YJ//-~
units: mg/L
RL: 0,005
Client ID Lab ID
RB17-0 715851
RB18-0-V 715856
MCL
5.0
5.0
Lead
Sample Date
Result Qualifier Analyzed
79.6 5/14/98
59.8 5/14/98
RL=Reporting Limit
MCL=Maximum Contaminant Level
U=Not detected at specified reporting limits
Analytical Services Laboratory 2300 NW Walnut Blvd., Corvallis, OR 97330-3538 (541) 752-4271
Corvafiis Office P.O. Box 428, Corvallis, OR 97339-0428 Fax No. (541) 752-0276